Aqueous Corrosion Equipment
2-Liter Autoclave with Sample Holders
- 316 Stainless Steel
- Maximum allowable working pressure: 379 bar at 343 °C (5,500 psi at 650 °F)
- Sample holder can hold and insulate up to 24 samples
- Any sample with a 11/64″ hole can be held by the sample holder
2.75-Liter Autoclave with sample Holders
- 316 Stainless Steel
- 1-Gallon capacity; 360 °C (680 °F); up to 200 bar (2901 psi)
- Sample holder can hold and insulate up to 32 samples
5-Liter Windowed Autoclave (cost: 2.69 $/hour for outside users)
- 316 Stainless Steel
- Maximum operation temperature and pressure: 360 °C (680 °F) and 200 bar (2901 psi)
- Three sapphire windows
- Cu/Cu2O/ZrO2 reference electrode for Electrochemical Impedance Spesctroscopy
Recirculation Loop
- 316 Stainless Steel construction
- System operating temperature: room temperature to 400 °C (70 °F to 752 °F)
- Maximum system operating pressure: 210 bar (3,045 psi)
- Maximum system flow rate: 6 liters per hour
- Can be used with the 2.75-Liter or 5-Liter Autoclave
Includes:
- Conductivity, dissolved oxygen, and dissolved hydrogen monitoring
- 150-mL chemical injection reservoir and pump
- Two ion exchangers
- 10-Liter mixing tank
- 20-Liter storage tank
UV source
- 200-Watt mercury short arc lamp with 2000-hour guaranteed lifetime
- High-temperature light guide for use with 5-Liter Windowed Autoclave
Sample Preparation Equipment
Polishing
- Allied Manual Grinder/Polisher
- Allied Autopolisher
- Struers Autopolisher
- Struers twin-jet electropolisher for lamella preparation
- Vibratory polisher
- Allied automatic epoxy hot-mount
Cutting
- Allied high speed saw
- Allied low-speed saw
Molten Salt Equipment
Laser Induced Breakdown Spectrometer (LIBS)
- Measure concentration of impurities in molten salt samples.
UV- Vis Spectrometer
- Fiber coupled into glovebox for in-situ spectroscopic measurements of salts
- Measures concentration of fluorine and chlorine ions through used of tracer dopant
Purification
- Walk in fume hood for hydro-fluoro purification of fluoride salts
- Vacuum purifier for chloride and fluoride salts