Laboratory Equipment

Aqueous Corrosion Equipment

2-Liter Autoclave with Sample Holders

  • 316 Stainless Steel
  • Maximum allowable working pressure: 379 bar at 343 °C (5,500 psi at 650 °F)
  • Sample holder can hold and insulate up to 24 samples
  • Any sample with a 11/64″ hole can be held by the sample holder

2.75-Liter Autoclave with sample Holders

  • 316 Stainless Steel
  • 1-Gallon capacity; 360 °C (680 °F); up to 200 bar (2901 psi)
  • Sample holder can hold and insulate up to 32 samples

5-Liter Windowed Autoclave (cost: 2.69 $/hour for outside users)

  • 316 Stainless Steel
  • Maximum operation temperature and pressure: 360 °C (680 °F) and 200 bar (2901 psi)
  • Three sapphire windows
  • Cu/Cu2O/ZrO2 reference electrode for Electrochemical Impedance Spesctroscopy

Recirculation Loop

  • 316 Stainless Steel construction
  • System operating temperature: room temperature to 400 °C (70 °F to 752 °F)
  • Maximum system operating pressure: 210 bar (3,045 psi)
  • Maximum system flow rate: 6 liters per hour
  • Can be used with the 2.75-Liter or 5-Liter Autoclave

Includes:

  • Conductivity, dissolved oxygen, and dissolved hydrogen monitoring
  • 150-mL chemical injection reservoir and pump
  • Two ion exchangers
  • 10-Liter mixing tank
  • 20-Liter storage tank

UV source

  • 200-Watt mercury short arc lamp with 2000-hour guaranteed lifetime
  • High-temperature light guide for use with 5-Liter Windowed Autoclave

Sample Preparation Equipment

Polishing

  • Allied Manual Grinder/Polisher
  • Allied Autopolisher
  • Struers Autopolisher
  • Struers twin-jet electropolisher for lamella preparation
  • Vibratory polisher
  • Allied automatic epoxy hot-mount

Cutting

  • Allied high speed saw
  • Allied low-speed saw

 

Molten Salt Equipment

Laser Induced Breakdown Spectrometer (LIBS)

  • Measure concentration of impurities in molten salt samples.

UV- Vis Spectrometer

  • Fiber coupled into glovebox for in-situ spectroscopic measurements of salts
  • Measures concentration of fluorine and chlorine ions through used of tracer dopant

Purification

  • Walk in fume hood for hydro-fluoro purification of fluoride salts
  • Vacuum purifier for chloride and fluoride salts